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July 2008


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Combo-Vac Pumps


We have reduced prices of Combo-Vac pumps. See new prices in red below.

All Combo-Vacs consist of an ion pump, cryoshroud and sublimation pump assembly together with the appropriate cooling mechanism, control units, cables, internal heaters, 6 spare titanium sublimation filaments, and 2 UHV copper gaskets. Bolt the Combo-Vac to your system in any position, rough it down, and it's ready for operation.

Features

  • Ideal for vacuum applications where many different gases must be pumped.
  • Combo-Vacs integrate three standard components in one unit for selective pumping: an ion pump, a cooling unit, and a titanium sublimator.
  • High speed, filament-type titanium sublimator/baffle assembly works at a constant current setting for reliable repetitive operation. Four separate, spiral titanium alloy filaments are incorporated in the sublimator assembly to allow continuous pumping over a 120-hour period. cycling the operation extends sublimator assembly life proportionally.
  • Replaceable noble ion pumps with demountable high-voltage feedthrough.
  • Can be supplied with diode, hydrogen diode, or triode elements in a range of sizes. Please contact the factory for custom details.
  • Pumping port(s) are fitted with metal gasketed flange and are blanked off for bakeout and shipment.
  • Separate power supplied for selective operation of sublimator and noble ion pump(s).
  • Stainless steel construction.
  • Internal bakeout heaters.
  • Mounting brackets are attached to pump body for assembly and support.
  • Liquid nitrogen/water shroud standard.
  • Operates in any position.

What is a Combo-Vac Pump?

Combo-Vac pumps are a combination of titanium sublimation pumps and ion pumps in one cryo-cooled package. (Model COV-500 is an exception, as it has an integral water-cooled jacket rather than a cryoshroud.) They are often used in factory processing of high power vacuum tubes, X-ray sources, etc. It is well suited to the gases evolved by such devices in their initial processing. They are tremendously cost-effective for certain applications, i.e., where reliable, clean, contaminant-free pumping is a major consideration. Their high speed is the result of the ability of a freshly deposited titanium film in vacuum to chemisorb such gases as oxygen, nitrogen, water vapor, carbon monoxide, and carbon dioxide. When the walls on which titanium is deposited are water-cooled, speeds of 40 to 90 l/sec (depending upon gas species) for each square inch of substrate are obtained. Thus total pump speeds can be quite large for large deposition chambers. The ion pumps handle gases that are not pumped by the sublimation pump--more about this later.

Because you control the rate at which titanium is deposited on the walls, you can adjust pumping speeds to suit your needs. For example, if you must pump down to a certain pressure before starting a process, you can read that pressure more quickly by increasing the sublimation rate. If your process liberates gas, you will be able to speed the process with more speed at your disposal. Conversely, when the system is not in active use, the ion pump alone will maintain it at a low pressure indefinitely, thus conserving the titanium supply of the sublimation pump.

At this point, you might have a question about the ion pump: Since its speed is so much lower than that of the sublimation pump, why include it at all? One reason has already been mentioned. It's a reliable way to maintain a holding vacuum when the system is not in active use. The most important reason, however, is the noble ion pump's ability to pump the non-getterable gases such as methane and the noble gases. Since these gases are generally present in small quantities in most systems, a small ion pump is able to handle the load, providing it is specially designed to pump noble gases. Caution: If your process produces large quantities of non-getterable gases, this will determine the size of ion pump needed.

All Combo-Vacs use the SB-1000 sublimator assembly with a PS-500 control unit. The sublimator assembly holds four separate spiral titanium filaments, each with 1.5 grams of usable titanium. In normal operations, power is supplied to the filament for 90 seconds and then removed for an interval. The OFF interval is continuously selectable in the range of 2 to 120 minutes by means of a front panel control knob.

Pumping results are better with cyclic operation than with continuous operation. One reason has to do with the characteristics of heated surfaces in vacuum. The power dissipated has two undesirable effects. One is that it causes outgassing of interior substrates just as a bakeout does though in lesser degree. The second is the formation of methane at the hot filament. This is thought to be a catalyzed reaction between hydrogen or water vapor and carbon or carbon dioxide at the hot filament. Because methane is not pumped by the sublimator, it must be pumped by the ion pump. Obviously, intermittent operation produces less methane and less work for the sputter ion pump. What is observed during operation of the sublimation pump is a brief pressure rise as the filament comes up to sublimation temperature, followed by a gradual decline in pressure as the fresh titanium deposits and cools at the substrate. When the power is removed from the filament, the pressure will generally drop by an order of magnitude. No new titanium will be needed until the pressure begins to rise again. This last period of time is dependent on the rate of gas evolution in the system but is usually within the range of the sublimator control unit timer.

COV-500
The model COV-500 is the smallest combination pump offered by Thermionics. It has an 8" O.D., 6" I.D., UHV flanged pumping port. A reducing flange can be used to interface the pump with a manifold or with small individual devices. The pump operates in any position and is easily disassembled for cleaning and/or replacement of elements. This pump uses a water-cooled shroud.
COV-750
The model COV-750 offers an increase in speed and throughput for two reasons. First, there are 4 noble diode* pump elements available to handle a larger throughput of non-getterable gases. Second, a liquid nitrogen cryoshroud is added. The lower temperature of the cryoshroud as a deposition surface improves the intrinsic speed of the pump. As is the case for all the Combo-Vacs, it is simple to operate and is field proven. It can be used in tube processing, vacuum deposition systems, ion accelerators, and surface research.
COV-1000
The COV-1000 is the pump of choice when the non-getterable gas load is larger than the COV-750 can comfortably handle.
As with the other Combo-Vacs, it is shipped complete with all the components needed to get your system operational. You simply remove the blank-off flange and attach the Combo-Vac to your system. the control units are designed for rack mounting and are supplied with the high voltage and high current cables which attach to the pump. Filaments are already mounted in the sublimator assembly. Rough the system down, add LN2 to the cryoshroud (or use TLI model LNC-400 liquid nitrogen level controller), and turn on the control units. The final adjustment, made at operating pressure, is to adjust the sublimator interval so that the sublimator turns on after the pressure has risen 60 to 100% over its previous low value.
COV-2000
The COV-2000 offers additional throughput because the ion pump's capacity is double that of the COV-1000. That means additional speed for non-getterable gases. The overall system speed is increased by use of a larger flange and a shorter pump neck.

Ordering Information and Specifications

  COV-500 COV-750 COV-1000 COV-2000
Nom. nitrogen speed, l/sec (sublimator & ion pump) 500 plus 1000 1000 2000
Nom. air speed, l/sec (ion pump) 30/60 120 220 400
Max. argon speed, l/sec (ion pump) 7 28 56 112
Sublimator control unit PS-500 PS-500 PS-500 PS-500
Ion pump control unit PS-100 PS-350 PS-350 PS-1000
Number of internal heaters 2 4 4 8
UHV flange size (I.D./O.D. in inches) 6.0/8.0 6.0/8.0 6.0/8.0 6.0/8.0
Substrate coolant water LN2 LN2 LN2
Price $7,500. $8,950. $10,500. $13,450.
Shipping Weight (lbs.) 85 130 200 304

*Note: Due to the current shortage of Tantalum material, TLI may recommend a standard diode or triode pump to replace the noble diode pump. Please call our Applications Engineers at 1-800-962-2310 or 360-385-7707 for more information.


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